• 专利标题:   Preparation of magnetic nano-graphene oxide involves dispersing graphite raw material containing graphite powder and hydrogen peroxide in water and purifying, dispersing purified graphene oxide in water, dissolving ferrous sulfate in graphene oxide solution, filtering, washing and drying.
  • 专利号:   CN116040619-A
  • 发明人:   LI L, XU L, DU F, WANG Y, WU Q
  • 专利权人:   SICHUAN VOCATIONAL COLLEGE CHEM TECHNOLO
  • 国际专利分类:   C01B032/198
  • 专利详细信息:   CN116040619-A 02 May 2023 C01B-032/198 202347 Chinese
  • 申请详细信息:   CN116040619-A CN11656073 22 Dec 2022
  • 优先权号:   CN11656073

▎ 摘  要

NOVELTY - Preparation of magnetic nano-graphene oxide involves dispersing graphite raw material containing graphite powder, hydrogen peroxide and auxiliary grinding agent in the ratio of 1:1:1 in water and separating to obtain graphene oxide through combination of mechanical action and oxidation reaction and purifying obtained graphene oxide, and modifying graphene oxide and preparing magnetic nano-graphene oxide, dispersing purified graphene oxide in water to obtain graphene oxide solution, dissolving 16 %(W/V) ferrous sulfate in the graphene oxide solution and adding 0.003 g surfactant simultaneously, leaving still for 2 hours in air, dripping 2 mol/L sodium hydroxide under strong stirring condition to pH of more than 9 to obtain a black suspension of the reaction product, filtering the reaction product, washing with distilled water and drying. USE - Preparation of magnetic nano-graphene oxide. ADVANTAGE - The magnetic nano-graphene oxide has good toughness, short curing time, strong adhesive force, simple preparation method, and high mechanical strength. The ion-exchange resin has higher surface charge concentration and stronger ability to adsorb ions than graphene oxide, so as to realize adsorption and removal of heteroions with high removal amount.