• 专利标题:   Preparation of sodium ion battery titanium dioxide/graphene composite negative electrode material involves mixing graphene and deionized water, ultrasonic treating, adding titanium tetrachloride, stirring, ultrasonic treating, and reacting.
  • 专利号:   CN107785539-A
  • 发明人:   XIAO W, WANG H, ZHAO L, LIU J, YAN C
  • 专利权人:   INST METAL RES CHINESE ACAD SCI
  • 国际专利分类:   H01M004/36, H01M004/48, H01M004/583, H01M010/054
  • 专利详细信息:   CN107785539-A 09 Mar 2018 H01M-004/36 201825 Pages: 6 Chinese
  • 申请详细信息:   CN107785539-A CN10718324 25 Aug 2016
  • 优先权号:   CN10718324

▎ 摘  要

NOVELTY - Preparation of sodium ion battery titanium dioxide/graphene composite negative electrode material comprises mixing 20-100 mg graphene and 30-300 mL deionized water, ultrasonic treating for 30-180 minutes, adding 0.1-2.5 g titanium tetrachloride, stirring, ultrasonic treating for 30-120 minutes, feeding to hydrothermal synthesis reactor, reacting at 120-260 degrees C for 3-40 hours, quenching to room temperature, centrifuging, and freeze-drying. USE - Method for preparing sodium ion battery titanium dioxide/graphene composite negative electrode material. ADVANTAGE - The material has good cycle life, high electric conductivity, and improved physical and chemical stability and electrochemical performance. The preparation method is low cost and suitable for industrial production.