• 专利标题:   Preparing graphene transparent thin film comprises placing stainless steel metal substrate in vacuum heat treatment furnace, then dropping kerosene, cooling mixture in furnace, and coating acrylic acid polymer on the surface of substrate.
  • 专利号:   CN104291325-A, CN104291325-B
  • 发明人:   CHEN L, ZHANG C
  • 专利权人:   CHEN L, NANTONG HUASHENG PLASTIC PROD CO LTD
  • 国际专利分类:   C01B031/04, C23C016/02, C23C016/26, C01B032/186
  • 专利详细信息:   CN104291325-A 21 Jan 2015 C01B-031/04 201518 Pages: 4 Chinese
  • 申请详细信息:   CN104291325-A CN10464215 14 Sep 2014
  • 优先权号:   CN10464215

▎ 摘  要

NOVELTY - Preparing graphene transparent thin film comprises taking a stainless steel metal substrate, placing the substrate in a vacuum heat treatment furnace, then heating, carrying out chemical gas phase deposition of graphene thin film, keeping the temperature for 30-60 minutes, then dropping kerosene, cooling the dropped mixture in a furnace, coating acrylic acid polymer on the surface of stainless steel metal substrate, then drying to form a support layer, and peeling the support layer provided on the surface of substrate and then performing ultrasonic stripping. USE - The method is useful for preparing graphene transparent thin film (claimed). ADVANTAGE - The method is capable of economically preparing the graphene transparent thin film. DETAILED DESCRIPTION - Preparing graphene transparent thin film comprises taking a stainless steel metal substrate having a thickness of 0.3-1 mm and a roughness Ra of less than or equal to 0.01, placing the substrate in a vacuum heat treatment furnace at absolute vacuum degree of 1.3x 103-1.3 Pa and a heating speed of 15-20 degrees C/minutes, then heating, raising the temperature to 600-700 degrees C for 25-30 minutes, continuously raising the temperature to 1000-1100 degrees C, carrying out chemical gas phase deposition of graphene thin film, keeping the temperature for 30-60 minutes, then dropping kerosene at speed of 100-180 drops/minute, cooling the dropped mixture in a furnace to room temperature, coating acrylic acid polymer on the surface of stainless steel metal substrate having a thickness of 1.5-3 mu m, then drying to form a support layer, and peeling the support layer provided on the surface of substrate and then performing ultrasonic stripping.