• 专利标题:   Preparing chitosan-modified graphene oxide composite coating, comprises adding chitosan to acetic acid solution, adding graphene oxide, preparing product A and product B, centrifuging, preparing product D, washing and with epoxy modified polyurethane resin.
  • 专利号:   CN114806367-A, CN114806367-B
  • 发明人:   ZHANG H, WANG J, LIU P, LIU Q, SUN Y, CHEN R
  • 专利权人:   UNIV HARBIN ENGINEERING
  • 国际专利分类:   C09D175/04, C09D005/08
  • 专利详细信息:   CN114806367-A 29 Jul 2022 C09D-175/04 202284 Chinese
  • 申请详细信息:   CN114806367-A CN10327456 30 Mar 2022
  • 优先权号:   CN10327456

▎ 摘  要

NOVELTY - Preparing chitosan-modified graphene oxide composite coating comprises (i) (a) adding chitosan to 1-3% acetic acid solution to obtain homogeneous solution, i.e. product A, (b) adding graphene oxide to deionized water, uniformly mixing, and adding to product A to obtain product B, and (c) adjusting pH of product B to 4-6, uniformly stirring and centrifuging to obtain precipitate i.e. chitosan-modified graphene oxide (GC), (ii) (a) adding polyaspartic acid into deionized water, and mixing well to obtain C product, (b) adding GC to product C to dissolve, adjusting pH to 4-6, then adding glutaraldehyde to obtain product D, and (c) washing product D many times to obtain PASP-CS-GO, i.e. GCP, and (iii) mixing GCP with epoxy modified polyurethane resin to obtain GCP/EP-PU composite coating. USE - The method is useful for preparing chitosan-modified graphene oxide composite coating. ADVANTAGE - The method has simple preparation, high corrosion resistance and high self-repairing ability of prepared composite coating.