• 专利标题:   Method for producing highly dispersible graphene, involves adding rare earth solution with ethanol, immersing graphene oxide in rare earth modified solution, adding hydrated hydrazine solution to modified oxidized graphene dispersion.
  • 专利号:   CN106829934-A
  • 发明人:   LI Y, LI H, ZHAO Y, ZHU J, XU F, HU Y, YUAN H
  • 专利权人:   UNIV JIANGXI SCI TECHNOLOGY
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN106829934-A 13 Jun 2017 C01B-032/184 201750 Pages: 8 Chinese
  • 申请详细信息:   CN106829934-A CN10179878 23 Mar 2017
  • 优先权号:   CN10179878

▎ 摘  要

NOVELTY - The method for producing highly dispersible graphene, involves adding rare earth solution with ethanol as solvent, heating rare earth solution in water bath, adjusting pH to obtain rare earth modified solution, immersing graphene oxide in rare earth modified solution and dispersing to obtain modified oxidized graphene dispersion, adding hydrated hydrazine solution to modified oxidized graphene dispersion to obtain graphene solution, washing with anhydrous ethanol and deionized water, placing in oven and drying to obtain final product. USE - Method for producing highly dispersible graphene (claimed). ADVANTAGE - The environmentally-friendly method enables simple and economical production of highly dispersible graphene with excellent dispersion effect. DETAILED DESCRIPTION - The method for producing highly dispersible graphene, involves (S1) adding rare earth solution with ethanol as solvent, (S2) heating rare earth solution in water bath, adjusting pH of rare earth solution to 5-6 to obtain rare earth modified solution, (S3) immersing graphene oxide in 20-500 mg/mL rare earth modified solution at 18-22 degrees C and dispersing to obtain modified oxidized graphene dispersion, (S4) adding 80 %mass hydrated hydrazine solution to modified oxidized graphene dispersion to obtain graphene solution, (S5) washing with anhydrous ethanol and deionized water several times at 40-60 degrees C, until no rare earth ions are detected, placing in oven and drying to obtain highly dispersible rare earth modified graphene powder.