• 专利标题:   Preparing graphene oxide involves diluting graphene oxide solution by solvent and stirring, centrifuging at room temperature, stirring to obtain large-size graphene oxide and subjected to ultrasonic treatment at certain power.
  • 专利号:   CN107128907-A
  • 发明人:   ZHOU Z, HE X, HAN Z, YANG J, ZHOU C
  • 专利权人:   UNIV SHANGHAI SCI TECHNOLOGY
  • 国际专利分类:   C01B032/194, C01B032/198
  • 专利详细信息:   CN107128907-A 05 Sep 2017 C01B-032/194 201771 Pages: 8 Chinese
  • 申请详细信息:   CN107128907-A CN10308363 04 May 2017
  • 优先权号:   CN10308363

▎ 摘  要

NOVELTY - Preparing graphene oxide involves diluting the graphene oxide solution by solvent, where upper layer concentration of obtained graphene solution is 0.01-10mg/ml, stirring at speed of 2000-5000 revolution per minute (rpm) for 10-60 minutes to obtain large-size graphene oxide. The obtained product is centrifuged at speed of 6000-8000rpm at room temperature for 10-60 minutes. The upper layer of obtained solution is stirred at speed of 9000-11000rpm at room temperature for 10-60 minutes, where collected deposition portion is smaller size of graphene oxide. USE - Method for preparing graphene oxide (claimed). DETAILED DESCRIPTION - Preparing graphene oxide involves diluting the graphene oxide solution by solvent, where upper layer concentration of obtained graphene solution is 0.01-10mg/ml, stirring at speed of 2000-5000 revolution per minute (rpm) for 10-60 minutes to obtain large-size graphene oxide. The obtained product is centrifuged at speed of 6000-8000rpm at room temperature for 10-60 minutes. The upper layer of obtained solution is stirred at speed of 9000-11000rpm at room temperature for 10-60 minutes, where collected deposition portion is smaller size of graphene oxide. The upper liquid is the small size of the oxidation of small sized graphene. The obtained product is subjected to ultrasonic treatment at power of 100-900Watt for 10-240 minutes to obtain smaller size and more uniform graphene oxide.