• 专利标题:   Manufacturing a graphene oxide fiber by preparing graphene oxide dispersion containing graphene oxide sheets and dispersion medium, preparing graphene oxide gel fiber by spinning dispersion into coagulation bath, and drying the gel fiber.
  • 专利号:   WO2020032684-A1, KR2020017679-A
  • 发明人:   HAN T H, SUNG T H, EOM W S, HANTAEHEE, EOM W
  • 专利权人:   UNIV HANYANG IND COOP FOUND, UNIV HANYANG IUCFHYU
  • 国际专利分类:   D01D010/06, D01D005/06, D01F001/10, D01F009/12
  • 专利详细信息:   WO2020032684-A1 13 Feb 2020 D01D-005/06 202016 Pages: 19 English
  • 申请详细信息:   WO2020032684-A1 WOKR010075 09 Aug 2019
  • 优先权号:   KR092860

▎ 摘  要

NOVELTY - A graphene oxide fiber is manufactured by preparing a graphene oxide dispersion containing graphene oxide sheets and a dispersion medium; preparing a graphene oxide gel fiber (30a) by spinning the dispersion into a coagulation bath (200) containing a coagulating solvent which extracts the dispersion medium, a crosslinking agent which forms crosslinks between graphene oxide sheets and emulsifier for mixing the coagulating solvent and the crosslinking agent; and drying the graphene oxide gel fiber. USE - Manufacture of graphene oxide fiber. ADVANTAGE - The organic coagulation bath can control the shrinkage and drying speeds of graphene gel fiber during spinning in manufacture of a graphene oxide fiber using wet spinning. The manufactured graphene oxide fiber may exhibit excellent structural stability and facilitate hybridization with various materials. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for coagulation bath (200) for graphene wet spinning comprising a coagulating solvent which extracts a dispersion medium from a spun graphene oxide dispersion containing graphene oxide sheets and dispersion medium, a crosslinking agent which forms crosslinks between the graphene oxide sheets, and an emulsifier which mixes the coagulating solvent and the crosslinking agent. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic view of the process of manufacturing a graphene oxide fiber using a coagulation bath. Graphene oxide gel fiber (30a) Spinning solution (100) Nozzle (101) Coagulation bath (200)