• 专利标题:   Graphite alkene/prussian blue complex composite aerogel for electrochromic device comprises three-dimensional network structure by graphene sheet layers, where nanolevel prussian blue complex particle is attached to graphite layer.
  • 专利号:   CN102824883-A, CN102824883-B
  • 发明人:   CHEN L, ZHANG X
  • 专利权人:   BEIJING INST TECHNOLOGY
  • 国际专利分类:   B01J013/00, B01J020/20, B01J020/30, B01J027/26, C09K009/00, G01N027/30
  • 专利详细信息:   CN102824883-A 19 Dec 2012 B01J-013/00 201344 Pages: 16 Chinese
  • 申请详细信息:   CN102824883-A CN10309317 27 Aug 2012
  • 优先权号:   CN10309317

▎ 摘  要

NOVELTY - A graphite alkene/prussian blue complex composite aerogel comprises three-dimensional network structure by graphene sheet layers, where prussian blue complex particle is in nanolevel which is attached to graphite layer. USE - Graphite alkene/prussian blue complex composite aerogel for electrochromic device (claimed). ADVANTAGE - The aerogel has large specific surface area, low density, and excellent conductivity. It has excellent hydrogen storage performance, hydrogen peroxide catalytic reduction performance and electrochromic performance. The method has simple operation and low cost, and is suitable for industrial production in large scale. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation method of the graphite alkene/prussian blue complex composite aerogel which comprises adding metal cyanide in graphene oxide suspension and dispersing to obtain suspension A; adding metal salt in aqueous solution containing reducing agent to obtain solution B; and ultrasonically and uniformly mixing suspension A and solution B, standing to obtain composite hydrogel, drying to obtain composite aerogel. Metal salt is iron ion (Fe3+, Fe2+), cobalt ion (Co2+), copper ion (Cu2+), nickel ion (Ni2+), zinc ion (Zn2+), manganese ion (Mn2+), gallium ion (Ga2+), iridium ion (Ir3+), or cadmium ion (Cd2+). Soluble metal salt is sulfate, nitrate, phosphate or chloride. The reducing agent is sodium borohydride, urea, sodium sulfide, hydroiodic acid, vitamin C, sodium bisulfite or amino acid.