• 专利标题:   Preparation of cellulose-based magnetic gas gel material involves formulating aqueous graphene oxide solution, using graphene oxide, stirring, dispersing, dropping aqueous crosslinking agent solution under stirring, and freeze-drying.
  • 专利号:   CN104479174-A, CN104479174-B
  • 发明人:   CHEN Y, LIN H, XIONG J, XU S
  • 专利权人:   UNIV SOOCHOW
  • 国际专利分类:   C08B013/00, C08J003/24, C08J009/28, C08K003/04, C08K003/22, C08L001/32, H01F001/42
  • 专利详细信息:   CN104479174-A 01 Apr 2015 C08L-001/32 201551 Pages: 23 Chinese
  • 申请详细信息:   CN104479174-A CN10762914 14 Dec 2014
  • 优先权号:   CN10762914

▎ 摘  要

NOVELTY - A cellulose-based magnetic gas gel material is prepared by formulating 0.01-10 wt.% aqueous graphene oxide solution, using graphene oxide and amphoteric cellulose at ratio of 1:10-10:1, stirring at 200-600 rpm to obtain amphoteric cellulose/graphene oxide binary composite liquid, ultrasonically dispersing ferroferric oxide in ethyl alcohol to obtain 0.1-10 wt.% ferroferric oxide ethyl alcohol solution, slowly adding ferroferric oxide ethyl alcohol solution, uniformly stirring to obtain ternary composite liquid, dropping aqueous crosslinking agent solution under stirring, and freeze-drying. USE - Preparation of cellulose-based magnetic gas gel material. ADVANTAGE - Product is low-cost, has high strength, characteristic, biological compatibility, loading ability, and surface activity and absorption capacity. DETAILED DESCRIPTION - A cellulose-based magnetic gas gel material is prepared by formulating 0.01-10 wt.% aqueous graphene oxide solution, using graphene oxide and amphoteric cellulose at ratio of 1:10-10:1, stirring at 200-600 rpm to obtain amphoteric cellulose/graphene oxide binary composite liquid, ultrasonically dispersing ferroferric oxide in ethyl alcohol to obtain 0.1-10 wt.% ferroferric oxide ethyl alcohol solution, slowly adding ferroferric oxide ethyl alcohol solution to binary composite liquid, uniformly stirring to obtain amphoteric cellulose/graphene oxide/ferroferric oxide ternary composite liquid, using 0.1-2 wt.% aqueous crosslinking agent solution, dropping aqueous crosslinking agent solution to ternary composite liquid under stirring, continuously stirring for 1-60 minutes to obtain viscous graphene oxide/ferroferric oxide ternary compound, and freeze-drying in which density of product is 0.1-40 mg/cm3 in which ratio of ferroferric oxide and amphoteric cellulose is 1:10-1:200 and ratio of crosslinking agent and amphoteric cellulose is 1:50-1:400. DESCRIPTION OF DRAWING(S) - The drawing shows a scanning electric microscope image of cellulose-based magnetic gas gel material.