• 专利标题:   Preparation of graphene oxide polymerized titanium dioxide involves pouring metatitanic acid to graphene oxide suspension, adding hydrogen peroxide, heating titanium oxide-graphite oxide sol and precipitating product.
  • 专利号:   CN106698506-A
  • 发明人:   LIU T, REN Y, FANG Y, CAO P, LIU Y, YANG S
  • 专利权人:   CHONGQING ZHONGDING SANZHENG TECHNOLOGY
  • 国际专利分类:   B01J021/18, C01B032/198, C01G023/053
  • 专利详细信息:   CN106698506-A 24 May 2017 C01G-023/053 201752 Pages: 5 Chinese
  • 申请详细信息:   CN106698506-A CN11190460 21 Dec 2016
  • 优先权号:   CN11190460

▎ 摘  要

NOVELTY - Metatitanic acid is poured to graphene oxide suspension. 30% Aqueous solution of hydrogen peroxide is added to mixture, stirred, and ammonia is dripped to mixture and stirred for 3-10 hours, to obtain titanium oxide-graphite oxide sol. The obtained titanium oxide-graphite oxide sol is maintained at 80-120 degrees C for 4-24 hours. Titanium oxide-graphite oxide sol is heated. The graphene oxide polymerized titanium dioxide is precipitated from solution, filtered and dried, to obtain graphene oxide polymerized titanium dioxide. USE - Preparation of graphene oxide polymerized titanium dioxide (claimed). DETAILED DESCRIPTION - A graphene oxide suspension is prepared. The metatitanic acid is poured to graphene oxide suspension. 30% Aqueous solution of hydrogen peroxide is added to mixture, stirred, and ammonia is dripped to mixture, and the pH is adjusted to 8.5-10 and stirred for 3-10 hours, to obtain titanium oxide-graphite oxide sol. The mass ratio of metatitanic acid, hydrogen peroxide solution and graphene oxide suspension is 5-7:40-60:100-105. The obtained titanium oxide-graphite oxide sol is maintained at 80-120 degrees C for 4-24 hours. Titanium oxide-graphite oxide sol is heated. The graphene oxide polymerized titanium dioxide is precipitated from solution, filtered and dried, to obtain graphene oxide polymerized titanium dioxide.