• 专利标题:   Preparing three-dimensional ordered porous nitrogen-doped graphene comprises performing ultrasonic dispersion, dissolving dopamine, mixing dopamine solution and GO dispersion liquid, dispersing and roasting PDA-rGO composite.
  • 专利号:   CN111252753-A
  • 发明人:   SHAO Z, TANG X, YANG L, HUANG H, QIN X
  • 专利权人:   CAS DALIAN CHEM PHYSICAL INST
  • 国际专利分类:   B82Y030/00, C01B032/184, H01M004/90
  • 专利详细信息:   CN111252753-A 09 Jun 2020 C01B-032/184 202050 Pages: 9 Chinese
  • 申请详细信息:   CN111252753-A CN11458592 30 Nov 2018
  • 优先权号:   CN11458592

▎ 摘  要

NOVELTY - Preparing three-dimensional ordered porous nitrogen-doped graphene comprises (a) performing ultrasonic dispersion of graphene oxide (GO) in water to obtain GO dispersion liquid, (b) dissolving dopamine (DA) in tris-hydroxymethylaminomethane-hydrochloric acid (Tris-HCl) solution to obtain a dopamine solution, where the concentration of the dopamine (DA) is 0.1-10 mmol/l, (c) mixing the dopamine solution and the GO dispersion liquid, dispersing them ultrasonically and stirring at 25-100 degrees C for 0.5-24 hours to obtain PDA-GO complex and (d) roasting the PDA-rGO composite under an inert atmosphere at 450-900 degrees C for 0.5-8 hours. USE - The graphene is useful as a catalyst or carrier in fuel cells and electrolytic cells (claimed). ADVANTAGE - The method is green and environmentally friendly, simple and easy to implement; has no special requirements for equipment; and is economical and easy to popularize and use. The graphene has broad application prospects in the fields of fuel cells and electrolytic cells. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for three-dimensional ordered porous nitrogen-doped graphene comprising specific surface area of the three-dimensional ordered porous nitrogen-doped graphene with 200-1000 g/m2, nitrogen-doping amount of 3-10 wt.%, pore diameter of 50 nm-20 mu m and pore volume of 0.1-5 cm3/g.