• 专利标题:   Making magnetic graphene oxide for waste water treatment, by adding ferric acetylacetonate and graphene oxide in octylamine and octanol solution, ultrasonically dispersing, performing high temperature reaction, cooling, magnetic separating.
  • 专利号:   CN103846076-A, CN103846076-B
  • 发明人:   BAI X, GU L, HUA Z, LIU X, FENG R, JI L
  • 专利权人:   UNIV HOHAI
  • 国际专利分类:   B01J020/20, B01J020/28, B01J020/30, C02F001/28, C02F001/62
  • 专利详细信息:   CN103846076-A 11 Jun 2014 B01J-020/20 201455 Pages: 11 Chinese
  • 申请详细信息:   CN103846076-A CN10513916 05 Dec 2012
  • 优先权号:   CN10513916

▎ 摘  要

NOVELTY - Preparation of magnetic graphene oxide, involves: adding ferric acetylacetonate and the graphene oxide in octylamine and octanol mix solution in ratio of 0.1-5 g:1 g:5-100 ml:10-200 ml, respectively; ultrasonically dispersing in reaction vessel for 10-300 minutes at a frequency of 40 KHz; performing high temperature reaction at 200-300 degrees C for 1-3 hours; cooling to room temperature; separating magnetic substance using magnetic separation; repeatedly washing with organic solvent, and then drying separated magnetic substance at 60-110 degrees C for 1-5 hours to obtain magnetic graphene oxide. USE - For preparation of magnetic graphene oxide (claimed) useful in waste water treatment. ADVANTAGE - The magnetic graphene oxide prepared by this method provides superparamagnetic and strong adsorption performance; can be used in waste water treatment; has good magnetic properties and adsorption capacity, and stable physical and chemical properties; and has low cost, and rapid separation and recovery characteristics. DETAILED DESCRIPTION - Preparation of magnetic graphene oxide, involves: adding ferric acetylacetonate and the graphene oxide in octylamine and octanol mix solution, where the ferric acetylacetonate, graphene oxide, octylamine and octanol are present in a ratio of 0.1-5 g:1 g:5-100 ml:10-200 ml; transferring the mixture to reaction vessel; ultrasonically dispersing for 10-300 minutes at a frequency of 40 KHz; performing a high temperature reaction at 200-300 degrees C for 1-3 hours; after completion of the reaction cooling to room temperature; separating the magnetic substance using magnetic separation; repeatedly washing with organic solvent, and then drying the separated magnetic substance at 60-110 degrees C for 1-5 hours; and finally obtaining the magnetic graphene oxide.