• 专利标题:   Flexible and self-supporting graphene oxide paper preparation for preparing glucose sensor, involves mixing soluble palladium-containing precursor and polyvinylpyrrolidone, and then diluting with deionized water with stirring ultrasonically.
  • 专利号:   CN108467029-A
  • 发明人:   LI Z, ZHU Z, SONG R
  • 专利权人:   UNIV SHANGHAI POLYTECHNIC
  • 国际专利分类:   C01B032/184, B22F009/24, G01N027/327, G01N027/48
  • 专利详细信息:   CN108467029-A 31 Aug 2018 C01B-032/184 201866 Pages: 10 Chinese
  • 申请详细信息:   CN108467029-A CN10633873 20 Jun 2018
  • 优先权号:   CN10633873

▎ 摘  要

NOVELTY - Flexible and self-supporting graphene oxide paper preparation involves mixing 2-20 ml 1 mg/ml soluble palladium-containing precursor and 5-2000 mg polyvinylpyrrolidone, and then diluting with 70 ml deionized water with stirring ultrasonically to obtain brown solution. The obtained mixed solution is heated in water bath at 80-100 degrees C with 2-30 ml 85 wt.% hydrazine hydrate solution with stirring for 0.5-3 hours. The reaction mixture is cooled at room temperature, and then dispersion ultrasonically for 0.5-3 hours. The ultrasonically dispersed solution is poured into a suction filter, and then vacuum-filtered by using a water filtration membrane having a pore size of 0.22-0.45 mu m. The filter is removed from the suction filter, left at room temperature for 10-15 hours, and then peeled off finally to obtain the flexible and self-supporting graphene oxide paper. USE - Method for preparing flexible and self-supporting graphene oxide paper for preparing glucose sensor (claimed). ADVANTAGE - The method prepares the flexible and self-supporting graphene oxide paper in a simple, cost-effective and eco-friendly manner with fast response to glucose, a wide linear response range, and high sensitivity. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic scanning electron microscopic image of the prepared flexible and self-supporting graphene oxide paper.