• 专利标题:   Preparation of silane graphene thermal conductive coating used for e.g. electric hot plates, involves adding silane to graphite, dispersing in dimethylformamide, adding activating agent and silane coupling agent, heating, and drying.
  • 专利号:   CN104557138-A
  • 发明人:   LIU Y, MIN Y, MO S, TONG S, WANG J, YANG W
  • 专利权人:   XINYUEHUA TECHNOLOGY HANGZHOU CO LTD, YANCHENG ZENGCAI TECHNOLOGY CO LTD, NANJING XINYUE MATERIAL TECHNOLOGY CO
  • 国际专利分类:   B05D007/14, C03C017/00, C04B041/80
  • 专利详细信息:   CN104557138-A 29 Apr 2015 C04B-041/80 201550 Pages: 9 Chinese
  • 申请详细信息:   CN104557138-A CN10341660 18 Jul 2014
  • 优先权号:   CN10341660

▎ 摘  要

NOVELTY - The preparation method of a silane graphene thermal conductive coating involves taking graphite as raw material and then improving oxidation to obtain modified graphene oxide, freeze-drying the modified graphene oxide to obtain lyophilized graphene oxide, adding silane to the lyophilized graphene oxide, dispersing the mixture in dimethylformamide solution, adding activating agent and oxygen radical to the mixture and then stirring, adding silane coupling agent to the mixture and then reacting, dissolving the mixture in an organic solvent and then heating, and drying. USE - The method is useful for preparation of silane graphene thermal conductive coating, which is useful for electric hot plates, electric heating kettle and electric knives. ADVANTAGE - The method enables preparation of silane graphene coating with excellent thermal conductivity and adsorption force. DETAILED DESCRIPTION - The preparation method of a silane graphene thermal conductive coating involves taking graphite as raw material and then improving oxidation using Hummers method to obtain modified graphene oxide, freeze-drying the modified graphene oxide to obtain lyophilized graphene oxide, adding silane to the lyophilized graphene oxide, uniformly mixing, dispersing the mixture in dimethylformamide solution, adding activating agent and oxygen radical to the mixture and then stirring, adding silane coupling agent to the mixture and then reacting to obtain silylated graphene oxide, dissolving the silylated graphene oxide in an organic solvent, spraying substrate, heating the mixture at high temperature, and drying.