• 专利标题:   Preparation of conductive agent-containing graphene used for anode of lithium-ion battery, involves adding slurry containing binder and solvent to mixer, coating slurry on copper foil, heating foil, and introducing conductive agent.
  • 专利号:   CN104393239-A, CN104393239-B
  • 发明人:   DAI T, SONG H, ZHOU P, ZHAO D
  • 专利权人:   DONGGUAN XIANGFENGHUA BATTERY MATERIALS, FUJIAN XIANGFENGHUA NEW ENERGY MATERIAL
  • 国际专利分类:   H01M004/04, H01M004/139, H01M004/62
  • 专利详细信息:   CN104393239-A 04 Mar 2015 H01M-004/139 201531 Pages: 9 Chinese
  • 申请详细信息:   CN104393239-A CN10534849 11 Oct 2014
  • 优先权号:   CN10534849

▎ 摘  要

NOVELTY - A slurry containing binder and solvent is added to a high-speed mixer and dispersed, to obtain cathode slurry. The slurry is coated on a cleaned copper foil and dried, to form slurry-coated copper foil as cathode. The solvent is removed by drying slurry. The slurry-coated copper foil is placed in reaction chamber, and the reaction chamber is sealed and evacuated. The foil is heated. The foil is cooled to room temperature. A conductive agent is introduced to processed copper-foil current collector, to obtain conductive agent-containing graphene. USE - Preparation of conductive agent-containing graphene used for anode of lithium-ion battery. ADVANTAGE - The method enables environmentally-friendly preparation of conductive agent-containing graphene having three-dimensional network structure by simple method, with high yield and reduced production equipment requirement. The lithium-ion-battery anode containing the conductive agent-containing graphene has high capacity and cycle characteristics. DETAILED DESCRIPTION - A slurry containing binder and solvent in ratio of 40-95:5-60:50-200 is added to a high-speed mixer and dispersed at rate of 500-5000 rpm for 1-4 hours, to obtain cathode slurry. The slurry is coated on a cleaned copper foil and dried, to form slurry-coated copper foil as cathode. The solvent is removed by drying slurry. The slurry-coated copper foil is placed in reaction chamber, and the reaction chamber is sealed and evacuated to l0-2 Pa for 10-60 minutes. The foil is heated at 500-1200 degrees C for 60-360 minutes, and heating is stopped. The foil is cooled to room temperature. A conductive agent is introduced to processed copper-foil current collector, to obtain conductive agent-containing graphene.