• 专利标题:   Preparation of porous graphene-based antibacterial material involves adding reducing agent to graphene oxide solution, hydrothermally reacting, cooling, mixing with silver-titanium dioxide antibacterial agent, and ultrasonically treating.
  • 专利号:   CN108651519-A
  • 发明人:   ZHAO L, TANG N, LENG J, SONG C, ZHONG Y, YU P, WANG X
  • 专利权人:   UNIV GUANGXI CHINESE MEDICINE
  • 国际专利分类:   A01N059/16, A01N059/00, A01P001/00
  • 专利详细信息:   CN108651519-A 16 Oct 2018 A01N-059/16 201883 Pages: 9 Chinese
  • 申请详细信息:   CN108651519-A CN10570685 05 Jun 2018
  • 优先权号:   CN10570685

▎ 摘  要

NOVELTY - Preparation of porous graphene-based antibacterial material involves dispersing titanium dioxide mesoporous beads and silver nitrate in deionized water, dissolving, stirring, adding a precipitating agent, heating resultant mixture at 60-90 degrees C for 5-30 minutes, ultrasonically processing, filtering, vacuum-drying, obtaining mixed crystal mesoporous silver-titanium dioxide antibacterial agent, ultrasonically dispersing graphene oxide in deionized water, obtaining an aqueous solution of graphene oxide, adding a reducing agent, stirring, dissolving, transferring resultant to an autoclave, hydrothermally reacting at 120-200 degrees C for 8-12 hours, cooling to room temperature, obtaining porous graphene solution, mixing with the antibacterial agent, adjusting pH to 9-11 using ammonia, ultrasonically treating for 60-90 minutes, vacuum-drying, washing with ethanol and deionized water, and vacuum-drying. USE - Preparation of porous graphene-based antibacterial material. ADVANTAGE - The method enables preparation of porous graphene-based antibacterial material having suppressed generation of agglomeration.