• 专利标题:   Preparing boron nitride coated graphene nanosheet comprises e.g. dissolving melamine and boric acid in anhydrous ethanol, then adding graphene nanosheet powder and surfactant, ultrasonicating, mechanically grinding and sintering.
  • 专利号:   CN108328585-A
  • 发明人:   MENG F, LI Y, YANG M, LIU X, DI J, ZHAO L
  • 专利权人:   UNIV HEBEI TECHNOLOGY
  • 国际专利分类:   C01B021/064, C01B032/182
  • 专利详细信息:   CN108328585-A 27 Jul 2018 C01B-021/064 201856 Pages: 10 Chinese
  • 申请详细信息:   CN108328585-A CN10412566 03 May 2018
  • 优先权号:   CN10412566

▎ 摘  要

NOVELTY - Preparing boron nitride coated graphene nanosheet comprises (i) dissolving 0.315-5.04 g melamine and 0.309-4.944 g boric acid in 20-40 ml anhydrous ethanol, stirring, adding 0.03-0.24 g graphene nanosheet powder and 1.5-2 g surfactant, ultrasonicating for 1.5-2.5 hours, stirring and filtering to obtain filtrate, where surfactant is polyvinylpyrrolidone K30, (ii) drying filtrate obtained in step (i) in a dry box at 40-65 degrees C for 8-12 hours, where drying box uses vacuum drying oven, and (iii) mechanically grinding dried product obtained in step (ii) under ammonia atmosphere and sintering at 900-1200 degrees C for 1.5-3.5 hours to obtain boron nitride-coated graphene nanosheet composite powder material. USE - The method is useful for preparing boron nitride coated graphene nanosheet.