• 专利标题:   Method for preparing spongy graphene/nickel cobalt sulfide composite material, involves weighing graphene oxide and sodium dodecylbenzenesulfonate, followed by transferring to high-pressure reaction vessel, centrifuging and calcining.
  • 专利号:   CN109003827-A
  • 发明人:   ZHENG Y, ZHAO W
  • 专利权人:   UNIV FUZHOU
  • 国际专利分类:   H01G011/24, H01G011/30, H01G011/36, H01G011/86
  • 专利详细信息:   CN109003827-A 14 Dec 2018 H01G-011/24 201915 Pages: 10 Chinese
  • 申请详细信息:   CN109003827-A CN10842895 27 Jul 2018
  • 优先权号:   CN10842895

▎ 摘  要

NOVELTY - A spongy graphene/nickel cobalt sulfide composite material preparing method involves weighing graphene oxide and sodium dodecylbenzenesulfonate, dissolving in deionized water, mixing and ultrasonicating to obtain a mixed solution, weighing sulfur and dispersing ultrasonically in n-octane to obtain a n-octane mixture, adding the n-octane mixture to the mixed solution and stirring magnetically to obtain a mixture, weighing nickel nitrate and cobalt nitrate, dissolving in deionized water, adding dropwise to the mixture and stirring magnetically to obtain a stirred solution. The stirred solution is transferred to Teflon (RTM: PTFE) lined stainless steel high-pressure reaction vessel, and the vessel is placed on the oil bath for reaction and stirred magnetically to obtain a product. The product is naturally cooled to room temperature, centrifuged, washed, vacuum dried and calcined the product to obtain the finished product. USE - Method for preparing spongy graphene/nickel cobalt sulfide composite material. ADVANTAGE - The method enables preparing spongy graphene/nickel cobalt sulfide composite material with large specific surface area and improved electrochemical performance.