• 专利标题:   Preparing defect-controlled pyridine nitrogen-doped porous graphene useful as fuel cell catalyst, comprises e.g. ultrasonically mixing cobalt salt, aqueous graphene oxide solution and ammonia water, reacting, centrifuging and heating.
  • 专利号:   CN108793126-A
  • 发明人:   WANG H, HUANG Q, CAO Y, YU H, PENG F
  • 专利权人:   UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   C01B032/184, C01B032/194, H01M004/96
  • 专利详细信息:   CN108793126-A 13 Nov 2018 C01B-032/184 201880 Pages: 9 Chinese
  • 申请详细信息:   CN108793126-A CN10569855 05 Jun 2018
  • 优先权号:   CN10569855

▎ 摘  要

NOVELTY - Preparing defect-controlled pyridine nitrogen-doped porous graphene comprises (i) ultrasonically mixing the cobalt salt, the aqueous graphene oxide solution and the ammonia water, reacting at a temperature of 60-80 degrees C, centrifuging the precipitate, and freeze-drying to obtain cobalt oxide-supported graphene oxide, (ii) heating the graphene oxide-supported graphene oxide in an inert atmosphere at a temperature of 500-700 degrees C, forming cobalt-reduced graphene oxide, cleaning and ultrasonically processing, and removing the metal, and (iii) subjecting the obtained porous graphene to nitrogen doping treatment in an ammonia gas atmosphere at a temperature of 600-800 degrees C. USE - The porous graphene is useful as fuel cell catalyst (claimed). ADVANTAGE - The porous graphene has uniform pore size distribution and uniform size, and has higher oxygen reduction catalytic performance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for defect-controlled pyridine nitrogen-doped porous graphene prepared by above mentioned method.