• 专利标题:   Growing graphene film on surface of copper powder, by heating copper powder or its mixture in chemical vapor deposition furnace to oxidation temperature, pre-oxidizing copper powder, continuously heating furnace to growth temperature, reducing surface of copper powder, growing graphene, and cooling.
  • 专利号:   CN113897590-A
  • 发明人:   CAO H, LV X, SHEN H, YANG J, MA Y
  • 专利权人:   ZHEJIANG CHINT ELECTRICS CO LTD, SHANGHAI XINCHI ENERGY TECHNOLOGY CO LTD
  • 国际专利分类:   C23C016/02, C23C016/26, C23C016/44
  • 专利详细信息:   CN113897590-A 07 Jan 2022 C23C-016/26 202225 Chinese
  • 申请详细信息:   CN113897590-A CN10573258 22 Jun 2020
  • 优先权号:   CN10573258

▎ 摘  要

NOVELTY - Growing graphene film on surface of copper powder involves: (S1) initially heating copper powder or copper powder mixture in a chemical vapor deposition furnace to an oxidation temperature, and pre-oxidizing the copper powder; (S2) continuously heating the chemical vapor deposition furnace to the growth temperature after pre-oxidation treatment is completed, and simultaneously reducing the surface of the copper powder and growing graphene; and (S3) cooling the growth product after the growth process is completed. USE - The method is useful for growing graphene film on surface of copper powder. ADVANTAGE - The method simplifies the growth process of the graphene film on the surface of the copper powder, ensures improved overall process efficiency, and utilizes pre-oxidation treatment combined with reduction and growth operations to reduce nucleation points, grain boundaries and defects on the surface of the copper powder, so that the grain size of the graphene film grown on the surface of the copper powder is large, generally reaching 5-10 microns, and improves the quality of graphene.