• 专利标题:   Preparing antibacterial antistatic graphene polyester spinning color masterbatch comprises e. g. taking raw materials, placing in a shear-dispersing mixer and dispersing to obtain homogeneous mixture.
  • 专利号:   CN110437477-A
  • 发明人:   ZHAO K, WANG B, YE Y, ZHOU Y
  • 专利权人:   SWOTO PROTECTION TECHNOLOGY CO LTD, ZHAO K
  • 国际专利分类:   C08J003/22, C08L067/00, D01F001/09, D01F001/10, D01F006/92
  • 专利详细信息:   CN110437477-A 12 Nov 2019 C08J-003/22 201990 Pages: 9 Chinese
  • 申请详细信息:   CN110437477-A CN10563595 26 Jun 2019
  • 优先权号:   CN10563595

▎ 摘  要

NOVELTY - Preparing antibacterial antistatic graphene polyester spinning color masterbatch comprises e. g. (i) taking 0.5-15 wt.% S type high temperature disperse dye, 0.3-4 wt.% graphene oxide powder, 5-10 wt.% dispersant, 0.1-2 wt.% thickening agent, 0.05-2 wt.% de-foaming agent and balance of water, placing in a shear-dispersing mixer and dispersing to obtain homogeneous mixture, injecting the homogeneous mixture into a ceramic nano- grinder for vacuum grinding, grinding into 300 nm, and stopping the grinding to obtain graphene dye color paste; (ii) adding the graphene dye color paste and the natural polyester into a high-speed kneader in the ratio of 1:4-10, heating and kneading to modify the coloring, and mixing at 170-230 degrees C to form colored polyester mixture; and (iii) smelting and co-extruding the colored polyester mixture in a twin-screw extruder, melting at 190-280 degrees C, at 120-380 revolutions/minute and processing into colored polyester melt by melt coloring. USE - The method is useful for preparing antibacterial antistatic graphene polyester spinning color masterbatch. ADVANTAGE - The method is simple and controllable and ensures water washing-resistant. DETAILED DESCRIPTION - Preparing antibacterial antistatic graphene polyester spinning color masterbatch comprises (i) taking 0.5-15 wt.% S type high temperature disperse dye, 0.3-4 wt.% graphene oxide powder, 5-10 wt.% dispersant, 0.1-2 wt.% thickening agent, 0.05-2 wt.% de-foaming agent and balance of water, placing in a shear-dispersing mixer and dispersing to obtain homogeneous mixture, injecting the homogeneous mixture into a ceramic nano- grinder for vacuum grinding, grinding into 300 nm, and stopping the grinding to obtain graphene dye color paste; (ii) adding the graphene dye color paste and the natural polyester into a high-speed kneader in the ratio of 1:4-10, heating and kneading to modify the coloring, and mixing at 170-230 degrees C to form colored polyester mixture; (iii) smelting and co-extruding the colored polyester mixture in a twin-screw extruder, melting at 190-280 degrees C, at 120-380 revolutions/minute and processing into colored polyester melt by melt coloring; (iv) smelting and co-extruding the colored polyester melt by a screw machine, drawing, water cooling, pelletizing, drying and packaging. An INDEPENDENT CLAIM is also included for antibacterial antistatic graphene polyester spinning color masterbatch is prepared by above mentioned method.