• 专利标题:   Coating of magnesium oxide on graphene-coated magnesium oxide involves mixing ethanol solution and graphene-coated magnesium oxide, adding magnesium alloy powder to uniform dispersion, filtering slurry, and sintering composite material.
  • 专利号:   CN104894419-A, CN104894419-B
  • 发明人:   LIU Y, YUAN Q, ZENG X
  • 专利权人:   UNIV NANCHANG
  • 国际专利分类:   C22C001/05, C22C023/00
  • 专利详细信息:   CN104894419-A 09 Sep 2015 C22C-001/05 201602 Pages: 8 Chinese
  • 申请详细信息:   CN104894419-A CN10088041 26 Feb 2015
  • 优先权号:   CN10088041

▎ 摘  要

NOVELTY - 250 ml or more Ethanol solution and 0.1-5 g graphene-coated magnesium oxide are mixed and ultrasonic-dispersed, to obtain uniform dispersion of graphene-coated magnesium oxide-ethanol mixture. 95 g or more AZ91 Magnesium alloy powder is added to uniform dispersion and ultrasonic-mechanical-stirred, to obtain slurry. The slurry is filtered, dried under vacuum, transferred to mold, and cold-pressed. Argon is supplied to composite material and sintered at 500-600 degrees C for 2-4 hours. The sintered composite is hot-extruded at 350-400 degrees C and heat-treated. USE - Coating of magnesium oxide on graphene-coated magnesium oxide (claimed). ADVANTAGE - The method enables economical and safe coating of magnesium oxide on graphene-coated magnesium oxide having excellent interfacial bond strength and grain refinement characteristics by simple method. DETAILED DESCRIPTION - 250 ml or more Ethanol solution and 0.1-5 g graphene-coated magnesium oxide are mixed and ultrasonic-dispersed for 1-2 hours, to obtain uniform dispersion of graphene-coated magnesium oxide-ethanol mixture. 95 g or more AZ91 Magnesium alloy powder with granularity of 325 or less is added to uniform dispersion of graphene-coated magnesium oxide-ethanol mixture and ultrasonic-mechanical-stirred for 1-3 hours, to obtain slurry. The slurry is filtered, dried under vacuum, transferred to mold, and cold-pressed at room temperature and pressure of 100-600 MPa. Argon is supplied to composite material and sintered at 500-600 degrees C for 2-4 hours. The sintered composite is hot-extruded at 350-400 degrees C and heat-treated.