• 专利标题:   Forming reduced graphene oxide thin film, by ultrasonically dispersing graphene oxide solution, coating the solution on indium tin oxide glass substrate, drying and placing substrate with graphene oxide film in a plasma discharge chamber.
  • 专利号:   CN104085884-A, CN104085884-B
  • 发明人:   LI J, WANG X, WEI J, WANG Q, CHEN C
  • 专利权人:   PLASMA PHYSICS INST CHINESE ACAD SCI
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104085884-A 08 Oct 2014 C01B-031/04 201503 Pages: 9 Chinese
  • 申请详细信息:   CN104085884-A CN10331508 11 Jul 2014
  • 优先权号:   CN10331508

▎ 摘  要

NOVELTY - Forming a reduced graphene oxide thin film, comprises (a) ultrasonically and uniformly dispersing graphene oxide solution, coating the solution on an electric conductive indium tin oxide glass substrate using a spin coater, and then drying at a temperature of 58-62 degrees C for 4-6 minutes to obtain a graphene oxide film, and (b) placing the substrate with graphene oxide film in a plasma discharge chamber, and regulating the parameters of the plasma discharge chamber to generate hydrogen and argon plasma mix that directly acts on the surface of the film. USE - The method is useful for forming reduced graphene oxide thin film (claimed). ADVANTAGE - The method is capable of rapidly and eco-friendly forming the reduced graphene oxide thin film with improved electrochemical properties and without any impurities. DETAILED DESCRIPTION - Forming a reduced graphene oxide thin film, comprises (a) ultrasonically and uniformly dispersing graphene oxide solution, coating the solution on an electrically conductive indium tin oxide glass substrate using a spin coater at a speed of 2950-3050 revolution per minutes (rpm) for 88-92 seconds, and then drying at 58-62 degrees C for 4-6 minutes to obtain a graphene oxide film, and (b) placing the substrate with graphene oxide film in a plasma discharge chamber, and regulating the parameters of the plasma discharge chamber to generate hydrogen and argon plasma mix that directly acts on the surface of the film to obtain a reduced graphene oxide thin film.