• 专利标题:   Synthesis of three-dimensional graphene-reinforced nickel based composite material involves taking glucose or citric acid, nickel nitrate hexahydrate and soluble salt template sodium chloride, mixing, and dissolving in deionized water.
  • 专利号:   CN106756167-A, CN106756167-B
  • 发明人:   HE C, FU K, ZHANG X, ZHAO N, SHI C, LIU E, HE F, LI Q, LI J
  • 专利权人:   UNIV TIANJIN, UNIV TIANJIN
  • 国际专利分类:   C22C001/05, C22C019/03
  • 专利详细信息:   CN106756167-A 31 May 2017 C22C-001/05 201749 Pages: 11 Chinese
  • 申请详细信息:   CN106756167-A CN11097238 02 Dec 2016
  • 优先权号:   CN11097238

▎ 摘  要

NOVELTY - Synthesis of three-dimensional graphene-reinforced nickel based composite material involves taking glucose or citric acid, nickel nitrate hexahydrate and soluble salt template sodium chloride, mixing, dissolving in deionized water, freeze-drying, grinding, synthesizing at 600-800 degrees C under argon and hydrogen mixed gas, cooling to room temperature, mixing, washing, removing sodium chloride, drying, dissolving nickel nitrate hexahydrate in anhydrous ethanol, dissolving prepared mixture, drying at 75 degrees C, vacuum drying at 55 degrees C, coating on three-dimensional graphene, and heating at 400-500 degrees C. USE - Method for synthesizing three-dimensional graphene-reinforced nickel based composite material. DETAILED DESCRIPTION - Synthesis of three-dimensional graphene-reinforced nickel based composite material comprises taking glucose or citric acid, nickel nitrate hexahydrate and soluble salt template sodium chloride, mixing, dissolving in deionized water, freeze-drying, grinding, synthesizing at 600-800 degrees C under argon and hydrogen mixed gas, cooling to room temperature, mixing, washing, removing sodium chloride, drying, dissolving nickel nitrate hexahydrate in anhydrous ethanol, dissolving prepared mixture, drying at 75 degrees C, vacuum drying at 55 degrees C, coating on three-dimensional graphene, heating at 400-500 degrees C, cooling, molding, and sintering at 700-800 degrees C. Mole ratio of nickel and carbon is 1:5-50.