• 专利标题:   Preparing nitrogen-doped molybdenum disulfide/graphene complex material useful as cathode material for lithium ion batteries, comprises e.g. adding graphene oxide in formaldehyde aqueous solution, obtaining dispersion B, mixing and reacting.
  • 专利号:   CN111106326-A
  • 发明人:   GUO J, LIAO S, LING F, ZHANG H, WANG S
  • 专利权人:   CHINA PETROLEUM CHEM CORP, SINOPEC DALIAN PETROLEUM PETROCHEMICAL
  • 国际专利分类:   H01M004/36, H01M004/38, H01M004/58, H01M004/587
  • 专利详细信息:   CN111106326-A 05 May 2020 H01M-004/36 202046 Pages: 12 Chinese
  • 申请详细信息:   CN111106326-A CN11262178 27 Oct 2018
  • 优先权号:   CN11262178

▎ 摘  要

NOVELTY - Preparing nitrogen-doped molybdenum disulfide/graphene complex material comprises (i) adding graphene oxide in formaldehyde aqueous solution to obtain dispersion A, (ii) adding melamine, molybdenum salt and sulfur powder into deionized water to obtain dispersion B, (iii) mixing dispersion A and dispersion B, heating to 50-80 degrees C, reacting for 10-60 minutes, adjusting the pH of the reaction solution to 7-9, heating to 100-200 degrees C, hydrothermally reacting for 12-24 hours, filtering and drying to obtain black solid powder, (iv) placing black solid powder obtained in step (iii) in microwave reaction chamber, heating with a microwave power of 300-1200W for 1-60min to obtain the nitrogen-doped molybdenum disulfide/graphene complex material. USE - The nitrogen-doped molybdenum disulfide/graphene complex material useful as cathode material for lithium ion batteries (claimed). DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for nitrogen-doped molybdenum disulfide/graphene complex material prepared by the above method.