• 专利标题:   Preparing composite material by mixing graphene, graphene microchip and pi-pi conjugated small molecule with water, re-dispersing, mixing foamed pre-dispersed graphene-graphene microchip with cyanate ester resin and vacuum degassing.
  • 专利号:   CN106893322-A, CN106893322-B
  • 发明人:   GAO F, BAI G, XIAO W, TIAN Y, ZHANG H, ZHANG Z, SHI W
  • 专利权人:   NAT CENT NANOSCIENCE TECHNOLOGY CHINA
  • 国际专利分类:   C08K003/04, C08K007/00, C08L063/00, C08L079/04, C08L079/08
  • 专利详细信息:   CN106893322-A 27 Jun 2017 C08L-079/04 201765 Pages: 12 Chinese
  • 申请详细信息:   CN106893322-A CN10212467 01 Apr 2017
  • 优先权号:   CN10212467

▎ 摘  要

NOVELTY - Preparing graphene/cyanate ester composite material by mixing graphene, graphene microchip and pi - pi conjugated small molecule with water and pre-dispersing, (b) subjecting the pre-dispersed aqueous solution to re-dispersion, cooling and drying to obtain the foamed pre-dispersed graphene-graphene microchip, (c) mixing the foamed pre-dispersed graphene-graphene microchip with cyanate ester resin and dispersing, (d) vacuum degassing the foamed pre-dispersed graphene-graphene microchip and cyanate ester resin, and (e) carrying out casting curing molding to obtain the composite material. USE - Method is useful for the preparation of graphene/cyanate ester composite material, which is useful in aerospace materials (all claimed). ADVANTAGE - The method enables the preparation of graphene/cyanate ester composite material with excellent electrical conductivity, thermal conductivity and mechanical property and low thermal expansion coefficient. DETAILED DESCRIPTION - Preparation method of graphene/cyanate ester composite material involves (a) mixing graphene, graphene microchip and pi - pi conjugated small molecule with water and then pre-dispersing, (b) subjecting the pre-dispersed aqueous solution to re-dispersion in an ice bath environment, cooling the obtained dispersion liquid under liquid nitrogen condition and drying to obtain the foamed pre-dispersed graphene-graphene microchip, (c) mixing the foamed pre-dispersed graphene-graphene microchip with cyanate ester resin and dispersing the graphene-graphene microchip into cyanate ester resin by stirring and grinding, (d) vacuum degassing the foamed pre-dispersed graphene-graphene microchip and cyanate ester resin, and (e) carrying out casting curing molding to obtain the graphene/cyanate ester composite material. An INDEPENDENT CLAIM is included for graphene/cyanate ester composite material prepared by the above method.