• 专利标题:   Graphene ink comprises water, and complex of non-volatile components including humic acid and reduced graphene oxide particles.
  • 专利号:   RU2018138062-A, RU2737798-C2
  • 发明人:   BASKAKOV S A, BASKAKOVA YU V, SHULGA N YU, SHULGA YU M
  • 专利权人:   GRAFENOKS LLC, GRAFENOKS CO LTD
  • 国际专利分类:   B82Y040/00, C01B032/194, C09D011/52
  • 专利详细信息:   RU2018138062-A 30 Apr 2020 C09D-011/52 202055 Pages: 1 Russian
  • 申请详细信息:   RU2018138062-A RU138062 30 Oct 2018
  • 优先权号:   RU138062

▎ 摘  要

NOVELTY - Graphene ink comprises 99-98 wt.% water, and 1-2 wt.% a complex of non-volatile components including 30-50% humic acid and 70-50% reduced graphene oxide particles. USE - Used as graphene ink. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing the graphene ink, comprising ultrasonic treatment of graphene oxide with its subsequent recovery, preferably by carrying out separation and purification of humic acid from acidic peat, then treating extracted humic acid with 30% aqueous ammonia to form ammonium humate, mixing the resulting solution of a water-soluble form of humic acid in reactor with an aqueous suspension of graphene oxide of a concentration of 5-10 mg/ml, mixing and adding 15-20 g a graphene oxide reducing agent e.g. glucose to the resulting mixture, heating the mixture to 70 degrees C and stirring until a black suspension is formed, then centrifuging the suspension and washing the precipitate with deionized water to remove glucose residues, and dispersing the resulting precipitate in water under ultrasonic irradiation at an operating frequency of 22 kHz and a power of 600 watts for 10 minutes.