• 专利标题:   Preparing lithium titanate/graphene nanomaterial, by dispersing titanium source in hydrogen peroxide, adding graphene oxide solution, reacting, adding lithium titanate/graphene oxide composite to ammonium bifluoride and sintering.
  • 专利号:   CN110600727-A
  • 发明人:   JIA M, CAO Y, LIU F, JIANG L
  • 专利权人:   UNIV CENT SOUTH
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/485, H01M004/62
  • 专利详细信息:   CN110600727-A 20 Dec 2019 H01M-004/485 202004 Pages: 6 Chinese
  • 申请详细信息:   CN110600727-A CN10948104 08 Oct 2019
  • 优先权号:   CN10948104

▎ 摘  要

NOVELTY - Method for preparing surface fluorinated lithium titanate/graphene composite nanomaterial, involves (a) uniformly dispersing graphene oxide in a solvent to obtain a graphene oxide solution, (b) uniformly dispersing a titanium source in an aqueous hydrogen peroxide solution containing a lithium source, adding the graphene oxide solution, uniformly mixing and reacting at 160-200 degrees C for 3 hours to obtain a lithium titanate/graphene oxide composite, (c) adding the lithium titanate/graphene oxide composite to an ammonium bifluoride solution and reacting at 160-200 degrees C for more than 3 hours to prepare a surface fluorinated lithium titanate/graphene oxide composite, and (d) carrying out high-temperature sintering on the surface fluorinated lithium titanate/graphene oxide composite under the protection of inert atmosphere containing hydrogen to obtain the finished product. USE - The method is useful for preparing surface fluorinated lithium titanate/graphene composite nanomaterial (claimed). ADVANTAGE - The composite nanomaterial is prepared by simple method and has excellent performance and excellent stability without using high-concentration acid and alkali as raw material.