• 专利标题:   Preparing metal nanoparticle comprises placing boron powder and metal in cleaned crucible, degassing, annealing single crystal metal sheet substrate, growing single layer of boron on substrate and depositing metal on boron-coated substrate by vacuum heating and forming metal dispersion.
  • 专利号:   CN115138854-A
  • 发明人:   DAI D, MA Z, ZHAO X, WANG H
  • 专利权人:   CAS DALIAN CHEM PHYSICAL INST
  • 国际专利分类:   B01J023/50, B22F009/12, B82Y030/00, B82Y040/00, C23C014/02, C23C014/14, C23C014/16, C23C014/26, C23C016/28
  • 专利详细信息:   CN115138854-A 04 Oct 2022 B22F-009/12 202200 Chinese
  • 申请详细信息:   CN115138854-A CN10338457 30 Mar 2021
  • 优先权号:   CN10338457

▎ 摘  要

NOVELTY - Preparing metal nanoparticle comprises (a) placing boron powder in a cleaned crucible, placing into a vacuum chamber for degassing, (b) placing the metal in the cleaned crucible, placing into the vacuum chamber for degassing, (c) placing a single crystal metal sheet (e.g. gold single wafer, a silver single wafer or a copper single wafer) substrate in a vacuum, annealing by vacuum argon ion bombardment sputtering, repeating the processing method of this operation to produce an atomically flat surface, (d) growing a single layer of boron on the substrate using molecular beam epitaxy method in vacuum and (e) depositing the metal on a boron-coated substrate by vacuum heating the metal in a crucible and forming a metal dispersion. USE - The method is useful for preparing metal nanoparticle. ADVANTAGE - The method has good controllable dispersion effect on gold, cobalt and iron; arranges the size of nano-particles in the scale range of high catalytic activity; directly uses nano-particles to carry out chemical vapor deposition controllable growth and grows ordered non-metallic nanostructures on the surface of boro-graphene and realize in-situ direct docking of semiconductor processing. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a metal nanoparticle supported on the borophene, which is obtained by the above method.