• 专利标题:   Preparing foam nickel-graphene three-dimensional porous electrode used as super capacitor, lithium ion battery or lithium-air battery electrode, involves cleaning nickel foam by glacial acetic acid, acetone and ethanol and washing.
  • 专利号:   CN106803461-A
  • 发明人:   YU X, YI Q, ZHONG J, ZHU J
  • 专利权人:   CHANGDE LIYUAN NEW MATERIAL CO LTD
  • 国际专利分类:   H01G011/24, H01G011/30, H01G011/36, H01G011/86, H01M004/36
  • 专利详细信息:   CN106803461-A 06 Jun 2017 H01G-011/24 201746 Pages: 10 Chinese
  • 申请详细信息:   CN106803461-A CN10833005 26 Nov 2015
  • 优先权号:   CN10833005

▎ 摘  要

NOVELTY - Preparing foam nickel-graphene three-dimensional porous electrode involves cleaning the nickel foam by glacial acetic acid, acetone and ethanol, washing with deionized water and drying, then preparing graphene oxide aqueous solution having concentration of 0.5-10 milligram/milliliter, and directly soaking the foam nickel into the graphene oxide aqueous solution for performing reduction reaction 30-80 degrees C for 2-12 hours. The graphene undergoes a reduction reaction during the immersion process and spontaneously deposited on the surface of foam nickel as a conductive substrate. USE - Method for preparing foam nickel-graphene three-dimensional porous electrode used as super capacitor, lithium ion battery or lithium-air battery electrode (claimed). ADVANTAGE - The method enables to prepare foam nickel-graphene three-dimensional porous electrode which is easy to process in a simple, time-saving and cost-effective manner, and suitable for large scale production. It has high specific surface area, and improves rate of reaction. DETAILED DESCRIPTION - Preparing foam nickel-graphene three-dimensional porous electrode involves cleaning the nickel foam by glacial acetic acid, acetone and ethanol, washing with deionized water and drying, then preparing graphene oxide aqueous solution having concentration of 0.5-10 milligram/milliliter, and directly soaking the foam nickel into the graphene oxide aqueous solution for performing reduction reaction 30-80 degrees C for 2-12 hours. The graphene undergoes a reduction reaction during the immersion process and spontaneously deposited on the surface of foam nickel as a conductive substrate to grow into graphene to form a foam nickel-graphene three-dimensional porous structure.