• 专利标题:   Preparation of molecularly imprinted sensor involves weighing chloroauric acid and graphene oxide, heating citric acid, polishing glassy carbon electrode, adding ethanol, N-ethyl-2-aminomethylpyrrolidine and metolachlor and reacting.
  • 专利号:   CN109060910-A
  • 发明人:   LI H, LI Z, LI D
  • 专利权人:   UNIV JINAN
  • 国际专利分类:   G01N027/30, G01N027/416, G01N027/48
  • 专利详细信息:   CN109060910-A 21 Dec 2018 G01N-027/30 201918 Pages: 7 Chinese
  • 申请详细信息:   CN109060910-A CN10995784 29 Aug 2018
  • 优先权号:   CN10995784

▎ 摘  要

NOVELTY - The preparation method of molecularly imprinted sensor involves weighing 85-92 %mass deionized water, 1-3 %mass chloroauric acid and 2-6 %mass graphene oxide, ultrasonically processing for 20 minutes, adding 3-8 %mass citric acid and then heating for 40 minutes, polishing glassy carbon electrode using polishing powder, distilled water and ethanol, adding 74-80 %mass ethanol, 6-10 %mass N-ethyl-2-aminomethylpyrrolidine, 6-10 %mass citraconic acid, 2-4 %mass metolachlor, 0.5-1.5 %mass diisocyanate and 3-5 %mass ammonium persulfate, reacting for 10-12 hours, soaking in ethanol and acetic acid mixed solution, dispersing in 1% chitosan-acetic acid solution and processing. USE - The method is useful for preparation of molecularly imprinted sensor. ADVANTAGE - The method enables preparation of molecularly imprinted sensor with high sensitivity, selectivity and specificity.