• 专利标题:   Method for preparing graphene coated-composite glass fiber that is utilized as thermally conductive filler, involves putting glass fiber into sodium hydroxide solution followed by processing, coating and drying.
  • 专利号:   CN104163578-A, CN104163578-B
  • 发明人:   FU W, LI X, ZOU X
  • 专利权人:   HANGZHOU HANGFU NEW MATERIAL TECHNOLOGY CO LTD, HANGZHOU HANGFU NEW MATERIAL TECHNOLOGY
  • 国际专利分类:   C03C025/44
  • 专利详细信息:   CN104163578-A 26 Nov 2014 C03C-025/44 201509 Pages: 8 Chinese
  • 申请详细信息:   CN104163578-A CN10350462 22 Jul 2014
  • 优先权号:   CN10350462

▎ 摘  要

NOVELTY - A graphene coated-composite glass fiber preparing method involves putting glass fiber into sodium hydroxide solution with concentration of 2-13 mol/l, processing the glass fibers with ultrasonic waves for 20-60 minutes to obtain roughened glass fiber surface, impregnating the glass fiber in 1-5 mass% silane coupling agent KH570 solution, water or dimethyl sulfoxide as solvent for 5-20 minutes, stirring the mixture slowly, and drying the fibers. The dried fibers are coated with graphene solution by spray or hydrothermal method followed by drying coated fibers. USE - Method for preparing graphene coated-composite glass fiber that is utilized as thermally conductive filler. ADVANTAGE - The method enables preparing graphene coated-composite glass fiber with enhanced thermal conductivity and mechanical strength compared to normal glass fiber and providing widely application as filler in market. DETAILED DESCRIPTION - A graphene coated-composite glass fiber preparing method involves putting glass fiber into sodium hydroxide solution with concentration of 2-13 mol/l, processing the glass fibers with ultrasonic waves for 20-60 minutes to obtain roughened glass fiber surface, impregnating the glass fiber in 1-5 mass% silane coupling agent KH570 solution, water or dimethyl sulfoxide as solvent for 5-20 minutes, stirring the mixture slowly, and drying the fibers. The dried fibers are coated with graphene solution by spray or hydrothermal method followed by drying coated fibers. The graphene solution comprises 0.3-1.2 mg/ml graphene, water, acetone and dimethyl sulfoxide.