• 专利标题:   Preparing kaolin-based porous material for absorbing mercury in coal-fired flue gas by taking kaolin powder into muffle furnace, adding activated kaolin to iron salt solution, pouring mixed solution into PTFE lining, separating mixed liquid into solid and liquid with centrifuge, and grinding.
  • 专利号:   CN113171747-A
  • 发明人:   YE Z, MENG X, ZHAO J, CHU R, ZHU Z, WU G, SONG S, LI X, FENG L, KONG H
  • 专利权人:   SHANXI GEMENG ZHONGMEI CLEAN ENERGYRESEA, UNIV CHINA MINING TECHNOLOGY BEIJING
  • 国际专利分类:   B01D053/02, B01J020/12, B01J020/28, B01J020/30
  • 专利详细信息:   CN113171747-A 27 Jul 2021 B01J-020/12 202175 Pages: 7 Chinese
  • 申请详细信息:   CN113171747-A CN10612917 02 Jun 2021
  • 优先权号:   CN10612917

▎ 摘  要

NOVELTY - Method for preparing kaolin-based porous material for absorbing mercury in coal-fired flue gas involves (a) taking 50 g kaolin powder into the muffle furnace and activating, (b) adding the activated kaolin to the prepared iron salt solution, immersing, and washing the immersed iron-based kaolin-based porous material (Fe-kaolin), (c) ultrasonically mixing the impregnated iron-based kaolin-based porous material, 120 ml deionized water and 60 ml absolute ethanol uniformly, and adding graphene oxide (GO) to the mixture and ultrasonically mixing, (d) pouring the mixed solution into a PTFE lining, placing in an autoclave, (e) separating the mixed liquid into solid and liquid with a centrifuge, and placing the obtained solid into a oven to dry, and finally grinding the dried solid into powder, and using Fe-kaolin-GO to adsorb the kaolin-based porous material of mercury in coal-fired flue gas. USE - Method used for preparing kaolin-based porous material for absorbing mercury in coal-fired flue gas. ADVANTAGE - The method efficiently removes mercury pollution in the flue gas of coal-fired power plants, obtains raw materials easily, is cost-effective and environmentally-friendly, has high added value, and has high economic comprehensive benefits. DETAILED DESCRIPTION - Method for preparing kaolin-based porous material for absorbing mercury in coal-fired flue gas involves (a) taking 50 g kaolin powder into the muffle furnace and activating at 700-800 degrees C for 2 hours, (b) adding the activated kaolin to the prepared iron salt solution with a pH of 4-5, immersing for 4-6 hours, and washing the immersed iron-based kaolin-based porous material (Fe-kaolin), (c) ultrasonically mixing the impregnated iron-based kaolin-based porous material, 120 ml deionized water and 60 ml absolute ethanol uniformly for 1 hour, and adding graphene oxide (GO) to the mixture and continuously ultrasonically mixing for 2 hours, (d) pouring the mixed solution into a PTFE lining, placing in an autoclave for 160-180 degrees C for 10 hours, (e) separating the mixed liquid into solid and liquid with a centrifuge, and placing the obtained solid into a 110 degrees C oven to dry for 2 hours, and finally grinding the dried solid into powder, and using Fe-kaolin-GO to adsorb the kaolin-based porous material of mercury in coal-fired flue gas.