• 专利标题:   Method for preparing porous controllable graphene for use in e.g. energy conversion application, involves mixing precursor with graphene solution to obtain dispersion, freeze-drying and performing microwave combustion treatment.
  • 专利号:   CN106744827-A, CN106744827-B
  • 发明人:   HUANG L, WAN J, ZHOU J
  • 专利权人:   UNIV HUAZHONG SCI TECHNOLOGY, UNIV HUAZHONG SCI TECHNOLOGY
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN106744827-A 31 May 2017 C01B-032/184 201747 Pages: 10 Chinese
  • 申请详细信息:   CN106744827-A CN11031835 22 Nov 2016
  • 优先权号:   CN11031835

▎ 摘  要

NOVELTY - Method for preparing porous controllable graphene, involves (i) mixing precursor with graphene solution in a mass ratio of 1:1-50:1 to obtain a dispersion, (ii) performing rapid freeze-drying treatment onto the dispersion for 5-10 minutes to obtain sample (a), (iii) freeze-drying the sample (a) to obtain a composite, (iv) subjecting the composite to a microwave combustion treatment to obtain sample (b), (v) washing sample (b) and drying to obtain porous graphene. USE - Method for preparing porous controllable graphene for use in energy conversion application, photocatalytic application, environmental protection application, and electronic equipment. ADVANTAGE - The prepared porous graphene has main pore diameter of 5- 200 nm, and excellent conductivity. The modification of the graphene is achieved quickly and simply.