• 专利标题:   Preparation of graphene by dissolving oxidized graphene into deionized water, and subjecting oxidized graphene solution to stripping, separating, and reducing by electric field.
  • 专利号:   CN102167312-A, CN102167312-B
  • 发明人:   ZHANG D
  • 专利权人:   UNIV TONGJI
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102167312-A 31 Aug 2011 C01B-031/04 201175 Pages: 7 Chinese
  • 申请详细信息:   CN102167312-A CN10103270 25 Apr 2011
  • 优先权号:   CN10103270

▎ 摘  要

NOVELTY - Preparation of graphene by dissolving 20-140 mu m oxidized graphene into deionized water to prepare 0.5-10 mg/ml oxidized graphene solution; adding solution to electrochemical container; stripping by alternating-current power of 10-150 V and 0-7 kHz at 20-80 degrees C for 10-120 minutes; separating oxidized graphene by alternating-current power at 5-100 V and 20-80 degrees C for 2-10 minutes; reducing oxidized graphene by alternating-current power at 1-50 V and 20-80 degrees C for 5-60 minutes; taking graphene by stripping using liquid transfer pipe; and separating and reducing from electrochemical container. USE - Preparation of graphene. ADVANTAGE - The method improves preparation efficiency and quality of graphene, reduces preparation cost, and is suitable for commercial production. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic diagram of a process for preparing graphene.