• 专利标题:   Preparing graphene/black phosphorus flexible fibrous super capacitor electrode material comprises using natural flake graphite as raw material, adopting improved Hummers method, grinding blocky BP with grinding rod and mixing graphene oxide dispersion liquid and dispersion liquid.
  • 专利号:   CN115101354-A
  • 发明人:   AI Y, LI T, LIU X, LIU Y, YOU J, SUN Y, DANG A
  • 专利权人:   UNIV NORTHWESTERN POLYTECHNICAL
  • 国际专利分类:   H01G011/24, H01G011/30, H01G011/36, H01G011/56, H01G011/84, H01G011/86
  • 专利详细信息:   CN115101354-A 23 Sep 2022 H01G-011/36 202306 Chinese
  • 申请详细信息:   CN115101354-A CN10626669 04 Jun 2022
  • 优先权号:   CN10626669

▎ 摘  要

NOVELTY - Preparing graphene/black phosphorus flexible fibrous super capacitor electrode material comprises (i) using natural flake graphite as raw material, adopting improved Hummers method to prepare graphene oxide dispersion; (ii) grinding blocky BP with a grinding rod to powdery particles with metallic color in a nitrogen glove box, taking the above-mentioned powdery particles and adding them to deoxygenated deionized water, and sonicating to obtain dispersion liquid of two-dimensional nanosheet BP; (iii) mixing graphene oxide dispersion liquid and BP dispersion liquid, and ultrasonically treating to obtain GO/BP composite solution; (iv) preparing GO/BP composite fiber; (v)dipping two rGO/BP composite fibers in PVA/H3PO4 gel electrolyte, drying at room temperature, placing in parallel on a PET film, and placed between the two fibers Cover with gel electrolyte and wait for it to dry. USE - The method is useful for preparing graphene/black phosphorus flexible fibrous super capacitor electrode material. ADVANTAGE - The method provides graphene/black phosphorus flexible fibrous super capacitor electrode material with good flexibility, good conductivity, environment-friendly and high specific capacitance, good mechanical property, capable of weaving, and good application potential in the wear-resistant electronic device and other fields.