• 专利标题:   Method for reducing nucleation density of graphene, involves passing gas into quartz tube to normal pressure after vacuuming and turning OFF heating and gas supply of tube furnace and cooling tube furnace to room temperature after growth of graphene is completed.
  • 专利号:   CN113387345-A
  • 发明人:   YUAN L
  • 专利权人:   UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   C01B032/184, C01B032/186, C30B029/02, C30B025/18
  • 专利详细信息:   CN113387345-A 14 Sep 2021 C01B-032/184 202180 Pages: 7 Chinese
  • 申请详细信息:   CN113387345-A CN10396336 13 Apr 2021
  • 优先权号:   CN10396336

▎ 摘  要

NOVELTY - The method involves using organic solvents and deionized water to clean the oil stains and other residues on the surface of the copper foil, and use compressed air to dry the surface. The dried copper foil is placed in a heating furnace for pre-oxidation. The heated copper foil is transferred to a quartz plate and placed in a tube furnace. The gas is passed into the quartz tube to normal pressure after vacuuming, and the reaction gas is introduced to grow graphene after the temperature is raised to 800-1000 degrees C. The heating and gas supply of the tube furnace is turned off and then cooled to room temperature after the growth is completed. USE - Method for reducing nucleation density of graphene. ADVANTAGE - The method is featured with simple operation and significant effect. The influence of different heating and annealing environments on the nucleation density of graphene is explored, so as to further reduce the nucleation density of graphene and increase the size of graphene single crystals on the basis of the method.