• 专利标题:   Modified polyacrylonitrile fiber film useful for absorbing lead ion in water, prepared by e.g. preparing mixture of polyacrylonitrile, chitosan and biochar, adding into mixture of dopamine and graphene oxide, stirring and electrospinning.
  • 专利号:   CN112452306-A
  • 发明人:   CHEN J, XU K
  • 专利权人:   CHEN J
  • 国际专利分类:   B01J020/26, B01J020/28, B01J020/30, C02F001/28, C02F101/20, D01F001/10, D01F006/54
  • 专利详细信息:   CN112452306-A 09 Mar 2021 B01J-020/26 202128 Pages: 8 Chinese
  • 申请详细信息:   CN112452306-A CN11238026 09 Nov 2020
  • 优先权号:   CN11238026

▎ 摘  要

NOVELTY - Modified polyacrylonitrile fiber film is claimed. The modified polyacrylonitrile fiber film is prepared by (i) adding polyacrylonitrile, chitosan, biochar and thioacetamide into solvent A, stirring ultrasonically for 30-50 minutes to obtain mixture I, where the mass ratio of polyacrylonitrile, chitosan, biochar and thioacetamide is 1:0.55-0.9:0.4-0.6:0.3-0.7, (ii) adding dopamine and graphene oxide into solvent B, stirring ultrasonically for 20-30 minutes to obtain mixture II, where the mass ratio of dopamine and graphite oxide is 1:0.23-0.45 and (iii) adding mixture II into mixture I, stirring, then adding ascorbic acid and 3% tris-buffer, stirring for 20 minutes to obtain spinning solution, transferring into electrospinning syringe pump and electrospinning to obtain final product, where the molar ratio of ascorbic acid to 3% tris-buffer is 0.1:0.06-0.09. USE - The modified polyacrylonitrile fiber film is useful for absorbing lead ion in water (claimed). ADVANTAGE - The modified polyacrylonitrile fiber film: has good removing rate to lead ion in water, the removing rate of the lead ion up to more than 95% even after circulating test ten times.