• 专利标题:   Preparing polyvinyl alcohol-graphene oxide nanocomposite hydrogel involves adding polyvinyl alcohol to deionized water, heating mixture to prepare polyvinyl alcohol aqueous solution, mixing graphene oxide aqueous solution and stirring.
  • 专利号:   CN106750379-A
  • 发明人:   SUN G
  • 专利权人:   QINGDAO ZHIXIN BIOTECHNOLOGY CO LTD
  • 国际专利分类:   C08J003/075, C08K003/04, C08K009/00, C08L029/04
  • 专利详细信息:   CN106750379-A 31 May 2017 C08J-003/075 201745 Pages: 4 Chinese
  • 申请详细信息:   CN106750379-A CN10820568 24 Nov 2015
  • 优先权号:   CN10820568

▎ 摘  要

NOVELTY - Preparing polyvinyl alcohol-graphene oxide nanocomposite hydrogel involves adding polyvinyl alcohol to deionized water, and heating mixture at 95 degrees C in a water bath for 2 hours to prepare a polyvinyl alcohol aqueous solution, and then mixing graphene oxide aqueous solution. The content of oxidized graphene in mixture is 5 wt.%, and size of graphene sheet is 2 mu m. The solution is stirred at 85 degrees C under magnetic stirring to form a homogeneous mixture with a stirring time of 0.5 hours and mixture is poured into a mold and placed in refrigerator at freezing temperature of -25 degrees C for 20 hours. USE - Method for preparing polyvinyl alcohol-graphene oxide nanocomposite hydrogel (claimed). ADVANTAGE - The method enables to prepare polyvinyl alcohol-graphene oxide nanocomposite hydrogel, which is stable under certain conditions and structure is maintained after melting. DETAILED DESCRIPTION - Preparing polyvinyl alcohol-graphene oxide nanocomposite hydrogel involves adding polyvinyl alcohol to deionized water, and heating mixture at 95 degrees C in a water bath for 2 hours to prepare a polyvinyl alcohol aqueous solution, and then mixing graphene oxide aqueous solution. The content of oxidized graphene in mixture is 5 wt.%, and size of graphene sheet is 2 mu m. The solution is stirred at 85 degrees C under magnetic stirring to form a homogeneous mixture with a stirring time of 0.5 hours and mixture is poured into a mold and placed in refrigerator at freezing temperature of -25 degrees C for 20 hours. The sample is removed and thawed at room temperature for 2-4 hours. The number of freeze thaw cycles is 7, and the resulting hydrogel is dried by freeze drying.