• 专利标题:   Brightener for hot melt coatings on road, is prepared by using e.g. microcrystalline polyethylene wax, 2,5-bis(5-tert-butyl-2-phenylazolyl)thiophene, vitamin E acetate, magnesium hydrogen sulfate, N-methylpyrrolidone and deionized water.
  • 专利号:   CN112980236-A
  • 发明人:   CHEN J, SONG Y, LIU J
  • 专利权人:   HENAN RUIQITE CHEM IND CO LTD
  • 国际专利分类:   B01J019/00, B01J019/18, B01J004/00, C09D011/03, C09D123/06, C09D007/61, C09D007/63, C09D007/65
  • 专利详细信息:   CN112980236-A 18 Jun 2021 C09D-007/65 202166 Pages: 17 Chinese
  • 申请详细信息:   CN112980236-A CN10267997 11 Mar 2021
  • 优先权号:   CN10267997

▎ 摘  要

NOVELTY - A brightener is prepared by using 20-32 pts. wt. microcrystalline polyethylene wax, 55-62 pts. wt. 2,5-bis(5-tert-butyl-2-phenylazolyl)thiophene, 2-5 pts. wt. vitamin E acetate, 1-2 pts. wt. magnesium hydrogen sulfate, 0.4-0.5 pt. wt. N-methylpyrrolidone, 3-5 pts. wt. butoctanol, and balance deionized water. USE - Brightener for hot melt coatings on road. ADVANTAGE - The brightener can be directly covered and painted on the hot-melt coating for the renovation of hot-melt coating products, especially the aging and faded hot-melt marking on the road. Direct application of the brightener can solve the problem of aging, fading and yellowing of high paints. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of the brightener, which involves (1) heating microcrystalline polyethylene wax to molten state, adding vitamin E acetate, N-methylpyrrolidone, and butoctanol in drops, stirring at 800-1000 rpm, placing in a temperature-controlled reactor to maintain a constant temperature, leaving still for 20-30 minutes, (2) dissolving magnesium hydrogen sulfate in deionized water, formulating into an aqueous solution with a concentration of 1-2%, adding 2,5-bis(5-tert-butyl-2-phenylazolyl)thiophene, filtering after soaking for 40-60 minutes, washing the resulting solution with water until it is neutral, drying, mixing the treated solution with the mixture obtained in step (1), stirring and dispersing at high speed for 40-50 minutes, and adding into grinder to grind until the particle size of the obtained slurry is 10 mu m or less.