• 专利标题:   Preparation of graphene/titania photocatalyst involves preparing graphite oxide, dissolving graphite oxide in water to obtain graphene oxide suspension, adding butyl titanate, absolute ethanol and glacial acetic acid, and stirring.
  • 专利号:   CN105964236-A
  • 发明人:   XU S, DONG K, LI R, ZHANG Y, ZHOU J
  • 专利权人:   UNIV TIANJIN POLYTECHNIC
  • 国际专利分类:   A62D101/28, A62D003/176, B01J021/06, B01J021/18
  • 专利详细信息:   CN105964236-A 28 Sep 2016 B01J-021/18 201677 Pages: 7 Chinese
  • 申请详细信息:   CN105964236-A CN10361682 27 May 2016
  • 优先权号:   CN10361682

▎ 摘  要

NOVELTY - The preparation of graphene/titania photocatalyst, involves (1) preparing graphite oxide by chemical process, dissolving obtained graphite oxide in water to obtain graphene oxide suspension, (2) adding butyl titanate, absolute ethanol and glacial acetic acid, mixing and stirring, dripping precursor mixture in graphene oxide suspension, transferring mixture to Teflon (RTM: PTFE) -lined reactor, heating reaction, cooling, washing, drying and grinding to obtain solid powder, (3) calcining resulting product in a muffle furnace, cooling out in the air, and grinding. USE - Preparation of graphene/titania photocatalyst (claimed). ADVANTAGE - The method enables preparation of graphene/titania photocatalyst with high specific surface area, high adsorption capacity and high photocatalytic activity, effectively removes volatile organic compound and improves degradation efficiency of acetone. DETAILED DESCRIPTION - The preparation of graphene/titania photocatalyst, involves (1) preparing graphite oxide by chemical process, dissolving obtained graphite oxide in certain amount of water for 1-3 hours to obtain certain concentration of graphene oxide suspension, (2) adding 8-13 ml butyl titanate, 30-50 ml absolute ethanol and 1-3 ml glacial acetic acid, mixing evenly and stirring, dripping precursor mixture in graphene oxide suspension, transferring mixture to Teflon (RTM: PTFE) -lined reactor, heating reaction, cooling, washing, drying and grinding to obtain solid powder, (3) calcining resulting product in a muffle furnace, cooling out in the air, and grinding.