• 专利标题:   Preparation of MFI molecular sieve/graphene nanosheet composite material involves mixing MFI molecular sieve and structural directing agent, adding graphene oxide dispersion liquid, reacting, water washing, centrifuging, and drying.
  • 专利号:   CN106904630-A, CN106904630-B
  • 发明人:   GUO X, DING H, BAI P
  • 专利权人:   UNIV TIANJIN, UNIV TIANJIN
  • 国际专利分类:   C01B032/198, C01B039/02
  • 专利详细信息:   CN106904630-A 30 Jun 2017 C01B-039/02 201761 Pages: 7 Chinese
  • 申请详细信息:   CN106904630-A CN10152458 15 Mar 2017
  • 优先权号:   CN10152458

▎ 摘  要

NOVELTY - Preparation of MFI molecular sieve/graphene nanosheet composite material involves uniformly mixing MFI molecular sieve and a structural directing agent (I) in an alkaline environment, adding graphene oxide dispersion liquid, magnetically stirring at 50-80 degrees C for 2-24 hours, adjusting pH of the resultant solution to 11-13, performing hydrothermal reaction at 100-190 degrees C for 24-240 hours, washing the resultant reaction product with water, centrifuging, and drying. USE - Preparation of MFI molecular sieve/graphene nanosheet composite material (claimed). ADVANTAGE - The method enables efficient preparation of MFI molecular sieve/graphene nanosheet composite material. The MFI molecular sieve can be coordinated with the graphene nanosheets. The graphene nanosheets promote the crystallization of the MFI molecular sieves. DETAILED DESCRIPTION - Preparation of MFI molecular sieve/graphene nanosheet composite material involves uniformly mixing MFI molecular sieve and a structural directing agent of formula (I) in an alkaline environment, adding graphene oxide dispersion liquid, magnetically stirring at 50-80 degrees C for 2-24 hours, adjusting pH of the resultant solution to 11-13, performing hydrothermal reaction at 100-190 degrees C for 24-240 hours, washing the resultant reaction product with water, centrifuging, and drying.