• 专利标题:   Method for preparing nitrogen-doped graphite alkene composite electrode material, involves obtaining oxidation graphene, carbon dioxide and product, and obtaining product mixed liquid by heating and drying alcohol after freezing.
  • 专利号:   CN105185606-A
  • 发明人:   MENG X, TANG S, XIE H
  • 专利权人:   UNIV NANJING
  • 国际专利分类:   H01G011/24, H01G011/30, H01G011/36, H01G011/86
  • 专利详细信息:   CN105185606-A 23 Dec 2015 H01G-011/86 201609 Pages: 11 English
  • 申请详细信息:   CN105185606-A CN10589125 14 Sep 2015
  • 优先权号:   CN10589125

▎ 摘  要

NOVELTY - A nitrogen-doped graphite alkene composite electrode material preparing method involves obtaining oxidation graphene concentration by adding oxidation graphite powder with deionized water. Carbon dioxide concentration is obtained by adding cobalt acetic acid to the obtained oxidation graphene concentration, followed by placing a reaction kettle containing reaction solution in water bath and obtaining product by heating and cooling the water bath. Product mixed liquid is obtained by cleaning an anhydrous ethyl alcohol with the deionized water and drying the alcohol after freezing the alcohol. USE - Method for preparing nitrogen-doped graphite alkene composite electrode material. ADVANTAGE - The method enables preparing nitrogen-doped graphite alkene composite electrode material with optimizing performance by charging and discharging circulation capacity to 94.2%. The method enables simplifying operation with low cost and easy control. DETAILED DESCRIPTION - A nitrogen-doped graphite alkene composite electrode material preparing method involves obtaining 0.5-4.0 mg/ml oxidation graphene concentration by adding 0.05-0.4 g oxidation graphite powder with 100 ml deionized water. 1-16 mm Carbon dioxide concentration is obtained by adding 8.75-14 mg cobalt acetic acid to the obtained oxidation graphene concentration, followed by stirring ammonia water by regulating pH value of 8.0-11 for 40 minutes, placing a reaction kettle containing reaction solution in 35 ml water bath after transferring 50 ml reaction solution to the reaction kettle, obtaining product by heating the water bath containing reaction solution at 100-240 degrees C low temperature for 4-16 hours, and cooling the water bath containing reaction solution by a centrifugal separation. Product mixed liquid is obtained at 70-85 degrees C under water bath condition by cleaning an anhydrous ethyl alcohol with the deionized water for 3-5 times, and drying the alcohol for 5-24 hours after freezing the alcohol.