• 专利标题:   Nitrogen doped reduced graphene oxide/cobalt titanate hybrid photocatalyst composite used in semiconductor industries, comprises cobalt titanate modified with nitrogen doped reduced graphene oxide dispersed in deionized water.
  • 专利号:   IN202231013238-A
  • 发明人:   PARIDA K, PARAMANIK L
  • 专利权人:   UNIV SIKSHA OANUSANDHAN
  • 国际专利分类:   B01J035/00, B01J037/02, H01G011/36, H01M004/36, H01M004/62
  • 专利详细信息:   IN202231013238-A 13 May 2022 B01J-035/00 202264 Pages: 25 English
  • 申请详细信息:   IN202231013238-A IN31013238 11 Mar 2022
  • 优先权号:   IN31013238

▎ 摘  要

NOVELTY - Nitrogen doped reduced graphene oxide/cobalt titanate hybrid photocatalyst composite, comprises cobalt titanate modified with 1 wt.% nitrogen doped reduced graphene oxide dispersed in 500 ml of deionized water. USE - The composite is useful for semiconductor industries. ADVANTAGE - The composite: exhibits high photocatalytic activity due to high light absorption capacity; provides photocatalytic performance evaluation towards hydrogen evolution and methyl orange degradation under visible light irradiation with high stability and durability; provides control and optimized route for synthesis; and provides easily controllable experimental conditions and photocatalytic efficiency of design material for photocatalytic hydrogen production and methyl orange degradation under visible light irradiation; photocatalyst with optimal ratio of 1 wt.% is effective in the visible region of the spectrum as compared to other photo catalysts of the series; is simple precipitation followed by reflux experimental methods under ambient conditions; and is highly resistive to photocorrision with high stability and reusability. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for synthesizing the photocatalyst composite, comprising (a) dispersing the cobalt titanate in the deionized water to obtain a solution, (b) adding stochiometric amount of graphene oxide and hydrazine monohydrate to form the nitrogen doped reduced graphene oxide added in the solution to obtain a reaction mixture, (c) refluxing the reaction mixture at a temperature of 80-90 degrees C for a period of 12 hours to obtain a refluxed material, and (d) centrifuging the refluxed material followed by multiple washing with deionized water and ethanol and further subjected to drying at a temperature of 75 degrees C overnight to obtain the photocatalyst composite.